p-Nitrophenyl-o-fluor-cinnaminsaeureester

Base Information

• Chemical Name: p-Nitrophenyl-o-fluor-cinnaminsaeureester
• CAS No.: 78335-18-9
• Molecular Formula: C₁₅H₁₀FNO₄
• Molecular Weight: 287.247
• Mol file: 78335-18-9.mol

Synonyms:p-Nitrophenyl-o-fluor-cinnaminsaeureester

Chemical Property of p-Nitrophenyl-o-fluor-cinnaminsaeureester

Chemical Property:

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Technology Process of p-Nitrophenyl-o-fluor-cinnaminsaeureester

There total 1 articles about p-Nitrophenyl-o-fluor-cinnaminsaeureester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ p-Nitrophenyl-o-fluor-cinnaminsaeureester (78335-18-9)

Guidance literature:

Cinnamoylchlorid, p-Nitrophenol;

DOI:10.1139/v75-070

Reference yield: 83.0%

p-Nitrophenyl-o-fluor-cinnaminsaeureester (78335-18-9) + 4-methyl-N-(1-phenylethylidene)benzenesulfonamide (24865-83-6) → (S)-4-(2-fluorophenyl)-6-phenyl-1-tosyl-3,4-dihydropyridin-2(1H)-one

Guidance literature:

With (5aR,10bS)-2-mesityl-5a,10b-dihydro-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazin-2-ium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 36h; enantioselective reaction; Inert atmosphere;

DOI:10.1002/anie.201303247

Reference yield:

p-Nitrophenyl-o-fluor-cinnaminsaeureester (78335-18-9) + 4-methyl-N-(1-phenylethylidene)benzenesulfonamide (24865-83-6) → 4-(2-fluorophenyl)-6-phenyl-1-tosyl-3,4-dihydropyridin-2(1H)-one

Guidance literature:

With 2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 36h; Inert atmosphere;

DOI:10.1002/anie.201303247