p-methoxybenzyl 2-deutero-2-oxoethyl ether

Base Information

Chemical Name:p-methoxybenzyl 2-deutero-2-oxoethyl ether
CAS No.:1255204-01-3
Molecular Formula:C₁₀H₁₂O₃
Molecular Weight:181.196
Hs Code.:

Synonyms:p-methoxybenzyl 2-deutero-2-oxoethyl ether

Suppliers and Price of p-methoxybenzyl 2-deutero-2-oxoethyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of p-methoxybenzyl 2-deutero-2-oxoethyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of p-methoxybenzyl 2-deutero-2-oxoethyl ether

There total 1 articles about p-methoxybenzyl 2-deutero-2-oxoethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1255204-00-2
p-methoxybenzyl 2,2-dideutero-2-hydroxyethyl ether

: 1255204-01-3
p-methoxybenzyl 2-deutero-2-oxoethyl ether

Guidance literature:: p-methoxybenzyl 2,2-dideutero-2-hydroxyethyl ether; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.5h;

With triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1021/ja106688j

Reference yield: 13.0%

: 1255204-01-3
p-methoxybenzyl 2-deutero-2-oxoethyl ether

: 4-(tert-butyldiphenylsilyloxy)butyltriphenylphosphonium bromide

: p-methoxybenzyl 6-(tert-butyldiphenylsilyloxy)-2-deutero-2-hexenyl ether

Guidance literature:: 4-(tert-butyldiphenylsilyloxy)butyltriphenylphosphonium bromide; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 0 - 20 ℃;

p-methoxybenzyl 2-deutero-2-oxoethyl ether; In tetrahydrofuran; toluene; for 2h;
DOI:10.1021/ja106688j