4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

Base Information

Chemical Name:4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide
CAS No.:1344686-07-2
Molecular Formula:C₁₄H₃ClF₉NO
Molecular Weight:407.623
Hs Code.:

Synonyms:4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

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Technology Process of 4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

There total 10 articles about 4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1300857-10-6
4-chloro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

: 1344685-95-5
4-chloro-2-fluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

: 1344686-07-2
4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

Guidance literature:: With tetrakis(acetonitrile)palladium bistriflate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; In 1-methyl-pyrrolidin-2-one; acetonitrile; at 120 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201102985

Reference yield: 66.0%

: 1300857-10-6
4-chloro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

: 1344686-07-2
4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

Guidance literature:: With tetrakis(acetonitrile)palladium bistriflate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; In 1-methyl-pyrrolidin-2-one; 4-methyl-1,2,3-trifluorobenzene; at 120 ℃; for 2h; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201102985

Reference yield:

: 434-64-0
perfluorotoluene

: 1344686-07-2
4-chloro-2,6-difluoro-N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium hydroxide / 1,4-dioxane; water / 80 °C

2: toluene / 28 h / 20 °C / Reflux

3: tetrakis(acetonitrile)palladium bistriflate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate / 1-methyl-pyrrolidin-2-one; 4-methyl-1,2,3-trifluorobenzene / 2 h / 120 °C / Inert atmosphere

With ammonium hydroxide; tetrakis(acetonitrile)palladium bistriflate; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; water; toluene; 4-methyl-1,2,3-trifluorobenzene;
DOI:10.1002/anie.201102985