N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

Base Information

Chemical Name:N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine
CAS No.:329310-35-2
Molecular Formula:C₄₀H₃₈N₆O₈
Molecular Weight:730.777
Hs Code.:

N<sup>6</sup>-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

Synonyms:N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

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Chemical Property of N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

Chemical Property:

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Technology Process of N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

There total 1 articles about N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: N⁶-benzoyl-8-bromo-5'-O-(4-methoxytrityl)adenosine

: 329310-35-2
N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

Guidance literature:: With triethylamine; In ethanol; at 70 ℃; for 48h;
DOI:10.1080/15257770008045452

Reference yield: 73.0%

: 108-24-7
acetic anhydride

: 329310-35-2
N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

: 329310-41-0
2',3'-di-O-acetyl-N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

Guidance literature:: In pyridine; at 22 ℃; for 18h;
DOI:10.1080/15257770008045452

Reference yield:

: 329310-35-2
N⁶-benzoyl-8-methoxycarbonylmethylamino-5'-O-(4-methoxytrityl)adenosine

: 329310-36-3
2',3'-di-O-acetyl-N⁶-benzoyl-8-methoxycarbonylmethylamino adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / pyridine / 18 h / 22 °C

2: Cl₂CHCOOH / CH₂Cl₂; methanol / 4 °C

With dichloro-acetic acid; In pyridine; methanol; dichloromethane;
DOI:10.1080/15257770008045452