3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate

Base Information

Chemical Name:3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate
CAS No.:946575-10-6
Molecular Formula:C₂₃H₃₉NO₅Si
Molecular Weight:437.652
Hs Code.:

Synonyms:3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate

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Chemical Property of 3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate

Chemical Property:

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Technology Process of 3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate

There total 6 articles about 3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₂₁NO₅

: 946575-10-6
3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.13 g / pyridine / CH₂Cl₂ / 3 h / 0 °C

2: 92 percent / imidazole; DMAP / CH₂Cl₂ / 3 h / 0 - 20 °C

3: hydrogen / Pd/C / methanol / 3 h / 20 °C / 760.05 Torr

4: 1.18 g / Na₂CO₃ / CH₂Cl₂; H₂O / 3 h / Heating

With pyridine; 1H-imidazole; dmap; hydrogen; sodium carbonate; palladium on activated charcoal; In methanol; dichloromethane; water;
DOI:10.1016/j.tetasy.2007.05.004

Reference yield:

: 946575-07-1
benzyl [(2S)-3-acetoxy-2-hydroxypropyl]-(3-acetoxy-propyl)carbamate

: 946575-10-6
3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / imidazole; DMAP / CH₂Cl₂ / 3 h / 0 - 20 °C

2: hydrogen / Pd/C / methanol / 3 h / 20 °C / 760.05 Torr

3: 1.18 g / Na₂CO₃ / CH₂Cl₂; H₂O / 3 h / Heating

With 1H-imidazole; dmap; hydrogen; sodium carbonate; palladium on activated charcoal; In methanol; dichloromethane; water;
DOI:10.1016/j.tetasy.2007.05.004

Reference yield:

: C₉H₁₉NO₃

: 946575-10-6
3-{[(2S)-3-acetoxy-2-tert-butyldimethylsilyloxypropyl](benzyl)amino}propyl acetate

Guidance literature:: Multi-step reaction with 6 steps

1: 3.15 g / Na₂CO₃ / CH₂Cl₂; H₂O / 3 h / 0 °C

2: p-TSA / methanol / 8 h / 20 °C

3: 1.13 g / pyridine / CH₂Cl₂ / 3 h / 0 °C

4: 92 percent / imidazole; DMAP / CH₂Cl₂ / 3 h / 0 - 20 °C

5: hydrogen / Pd/C / methanol / 3 h / 20 °C / 760.05 Torr

6: 1.18 g / Na₂CO₃ / CH₂Cl₂; H₂O / 3 h / Heating

With pyridine; 1H-imidazole; dmap; hydrogen; sodium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; dichloromethane; water;
DOI:10.1016/j.tetasy.2007.05.004