5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole

Base Information

Chemical Name:5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole
CAS No.:107355-85-1
Molecular Formula:C₁₈H₂₀Cl₂N₂O₄
Molecular Weight:399.274
Hs Code.:

Synonyms:5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole

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Chemical Property of 5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole

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Technology Process of 5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole

There total 1 articles about 5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35166-33-7
(5-methyl-isoxazol-3-yl)-methanol

: 107355-85-1
5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) THF, -78 deg C, 15 min, 2.) RT

2: 1.5 g / NaI, KOH / acetonitrile / 48 h / Heating

With potassium hydroxide; n-butyllithium; sodium iodide; In acetonitrile;
DOI:10.1021/jm00167a006

Reference yield: 70.0%

: 107355-85-1
5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole

: 331242-45-6
3-(bromomethyl)-5-[5-[2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy]-pentyl]-isoxazole

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

: 107355-85-1
5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-(hydroxymethyl)isoxazole

: 107355-90-8
2-<<<5-<5-<2,6-dichloro-4-(4,5-dihydro-2-oxazolyl)phenoxy>pentyl>-3-isoxazolyl>methoxy>methoxy>ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran / 48 h / Ambient temperature

2: LiOH / methanol; H₂O / 12 h / Ambient temperature

With lithium hydroxide; sodium hydride; In tetrahydrofuran; methanol; water;
DOI:10.1021/jm00167a006