N-(1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-triazol-4-ylmethyl)-4-methylbenzene sulfonamide

Base Information

Chemical Name:N-(1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-triazol-4-ylmethyl)-4-methylbenzene sulfonamide
CAS No.:1474027-10-5
Molecular Formula:C₁₈H₂₄N₄O₆S
Molecular Weight:424.478
Hs Code.:

Synonyms:N-(1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-triazol-4-ylmethyl)-4-methylbenzene sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-triazol-4-ylmethyl)-4-methylbenzene sulfonamide

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Technology Process of N-(1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-triazol-4-ylmethyl)-4-methylbenzene sulfonamide

There total 2 articles about N-(1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-triazol-4-ylmethyl)-4-methylbenzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5975-09-7
2,3-O-isopropylidene-β-D-ribofuranosyl-1-azide

: 55022-46-3
4-methyl-N-prop-2-ynylbenzenesulfonamide

: 1474027-10-5
N-(1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-triazol-4-ylmethyl)-4-methylbenzene sulfonamide

Guidance literature:: With monohydrate copper acetate; sodium carbonate; sodium L-ascorbate; In water; at 20 ℃; for 2h; Reagent/catalyst;
DOI:10.1080/07328303.2013.816852

Reference yield:

: 51970-31-1
(2R,3R,4S,5R)-2-azido-5-hydroxymethyl-tetrahydro-furan-3,4-diol

: 1474027-10-5
N-(1-(2,3-O-isopropylidene-β-D-ribofuranosyl)-triazol-4-ylmethyl)-4-methylbenzene sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: perchloric acid / acetone

2: monohydrate copper acetate; sodium carbonate; sodium L-ascorbate / water / 2 h / 20 °C

With perchloric acid; monohydrate copper acetate; sodium carbonate; sodium L-ascorbate; In water; acetone;
DOI:10.1080/07328303.2013.816852