1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct

Base Information

Chemical Name:1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct
CAS No.:1455481-87-4
Molecular Formula:C₂₁H₃₂F₅N₂P
Molecular Weight:438.464
Hs Code.:

Synonyms:1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct

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Chemical Property of 1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct

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Technology Process of 1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct

There total 3 articles about 1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1455481-82-9
2,2-difluoro-1,3-dimethyl-4-[4-(4-propylcyclohexyl)benzyl]imidazolidine

: 1455481-87-4
1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct

Guidance literature:: With trifluorophosphane; In diethyl ether; at -196 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: 1455481-68-1
1,3-dimethyl-4-[4-(4-propylcyclohexyl)benzyl]imidazolidin-2-one

: 1455481-87-4
1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / toluene / 12 h / 80 °C / Inert atmosphere

2: potassium fluoride / acetonitrile / 12 h / 85 °C / Inert atmosphere

3: trifluorophosphane / diethyl ether / -196 °C / Inert atmosphere

With potassium fluoride; oxalyl dichloride; trifluorophosphane; In diethyl ether; toluene; acetonitrile;
DOI:10.1016/j.tet.2013.07.062

Reference yield:

: 1455481-78-3
2-chloro-1,3-dimethyl-4-[4-(4-propylcyclohexyl)benzyl]-4,5-dihydro-1H-imidazol-3-ium chloride

: 1455481-87-4
1,3-dimethyl-4-[4′-(4-propylcyclohexyl)benzyl]imidazolin-2-ylidene-phosphorus(V) pentafluoride adduct

Guidance literature:: Multi-step reaction with 2 steps

1: potassium fluoride / acetonitrile / 12 h / 85 °C / Inert atmosphere

2: trifluorophosphane / diethyl ether / -196 °C / Inert atmosphere

With potassium fluoride; trifluorophosphane; In diethyl ether; acetonitrile;
DOI:10.1016/j.tet.2013.07.062