4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide
CAS No.:1310361-82-0
Molecular Formula:C₂₇H₃₇NO₄SSi
Molecular Weight:499.747
Hs Code.:

Synonyms:4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide

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Chemical Property of 4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide

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Technology Process of 4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide

There total 16 articles about 4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₂₇H₃₉NO₄SSi

: 1310361-82-0
4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 0 - 20 ℃; for 16h; Molecular sieve;
DOI:10.3762/bjoc.7.90

Reference yield: 28.0%

: C₂₇H₃₉NO₄SSi

: C₁₄H₂₂OSi

: 1310361-82-0
4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide

: 167847-61-2
4-methyl-N-[(5-methylfuran-2-yl)methyl]benzenesulfonamide

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 0 - 20 ℃; for 16h; Molecular sieve;
DOI:10.3762/bjoc.7.90

Reference yield:

: N-(3-{[tert-butyl(dimethyl)silyl]oxy}-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl)-4-methyl-N-[(5-methylfuran-2-yl)methyl]benzenesulfonamide

: 1310361-82-0
4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-{3-oxo-1-[(trimethylsilyl)ethynyl]non-8-en-1-yl}benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: water; acetic acid / tetrahydrofuran / 72 h / 0 - 20 °C

2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 16 h / 0 - 20 °C / Molecular sieve

With tetrapropylammonium perruthennate; water; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; 2: Ley oxidation;
DOI:10.3762/bjoc.7.90