N-{6-[(4-amino-6,7-dimethoxyquinazolin-2-yl)methylamino]hexyl}-3-formyl-N-methylbenzamide

Base Information

Chemical Name:N-{6-[(4-amino-6,7-dimethoxyquinazolin-2-yl)methylamino]hexyl}-3-formyl-N-methylbenzamide
CAS No.:328078-52-0
Molecular Formula:C₂₆H₃₃N₅O₄
Molecular Weight:479.579
Hs Code.:

Synonyms:N-{6-[(4-amino-6,7-dimethoxyquinazolin-2-yl)methylamino]hexyl}-3-formyl-N-methylbenzamide

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Chemical Property of N-{6-[(4-amino-6,7-dimethoxyquinazolin-2-yl)methylamino]hexyl}-3-formyl-N-methylbenzamide

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Technology Process of N-{6-[(4-amino-6,7-dimethoxyquinazolin-2-yl)methylamino]hexyl}-3-formyl-N-methylbenzamide

There total 2 articles about N-{6-[(4-amino-6,7-dimethoxyquinazolin-2-yl)methylamino]hexyl}-3-formyl-N-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75650-38-3
3-formylbenzoyl chloride

: 217973-01-8
6,7-Dimethoxy-N²-methyl-N²-(6-methylamino-hexyl)-quinazoline-2,4-diamine

: 328078-52-0
N-{6-[(4-amino-6,7-dimethoxyquinazolin-2-yl)methylamino]hexyl}-3-formyl-N-methylbenzamide

Guidance literature:: With triethylamine; In 1,4-dioxane; at 20 ℃; for 24h;
DOI:10.1021/jm000995w

Reference yield:

: 619-21-6
m-formylphenyl benzoic acid

: 328078-52-0
N-{6-[(4-amino-6,7-dimethoxyquinazolin-2-yl)methylamino]hexyl}-3-formyl-N-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / toluene / 1 h / Heating

2: Et₃N / dioxane / 24 h / 20 °C

With thionyl chloride; triethylamine; In 1,4-dioxane; toluene;
DOI:10.1021/jm000995w