5''-Hydroxy-cannabidiol

Base Information

Chemical Name:5''-Hydroxy-cannabidiol
CAS No.:53413-28-8
Molecular Formula:C₂₁H₃₀O₃
Molecular Weight:330.467
Hs Code.:

Synonyms:5''-Hydroxy-cannabidiol

Suppliers and Price of 5''-Hydroxy-cannabidiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5''-Hydroxy-cannabidiol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5''-Hydroxy-cannabidiol

There total 8 articles about 5''-Hydroxy-cannabidiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₆O₃

: 53413-28-8
5''-Hydroxy-cannabidiol

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 0.75h; Cooling with ice;

Reference yield:

: 74356-41-5
5-(3,5-dihydroxyphenyl)pentanoic acid

: 53413-28-8
5''-OH-cannabidiol

: C₂₁H₃₀O₃

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 18 - 60 °C / Inert atmosphere

2: toluene-4-sulfonic acid / tetrahydrofuran; dichloromethane / 2.5 h / 18 - 25 °C / Inert atmosphere

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acsmedchemlett.6b00009

Reference yield:

: 7311-34-4
3,5-dimethoxybenzaldehdye

: 53413-28-8
5''-OH-cannabidiol

: C₂₁H₃₀O₃

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / tetrahydrofuran / 3.08 h / 18 - 60 °C / Cooling with ice; Inert atmosphere

2: hydrogen; palladium(II) hydroxide; palladium 10% on activated carbon / methanol / 2 h / 18 - 25 °C / Inert atmosphere

3: hydrogen bromide / acetic acid / Reflux; Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 18 - 60 °C / Inert atmosphere

5: toluene-4-sulfonic acid / tetrahydrofuran; dichloromethane / 2.5 h / 18 - 25 °C / Inert atmosphere

With lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen bromide; hydrogen; palladium(II) hydroxide; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; acetic acid;
DOI:10.1021/acsmedchemlett.6b00009