B₂(NPh)4(B₂(NMe₂)2)2

Base Information

• Chemical Name: B₂(NPh)4(B₂(NMe₂)2)2
• CAS No.: 1290041-08-5
• Molecular Formula: C₃₂H₄₄B₆N₈
• Molecular Weight: 605.621
• Mol file: 1290041-08-5.mol

Synonyms:B₂(NPh)4(B₂(NMe₂)2)2

Chemical Property of B₂(NPh)4(B₂(NMe₂)2)2

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of B₂(NPh)4(B₂(NMe₂)2)2

There total 2 articles about B₂(NPh)4(B₂(NMe₂)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

dichlorobis(dimethylamino)diborane(4) (64541-76-0) + tetrakis(phenylamino)diborane(4) (4893-42-9) → B2(NPh)4(B2(NMe2)2)2 (1290041-08-5)

Guidance literature:

tetrakis(phenylamino)diborane⁽⁴⁾; With n-butyllithium; In tetrahydrofuran; at -78 ℃; Reflux;

dichlorobis(dimethylamino)diborane⁽⁴⁾; In tetrahydrofuran; diethyl ether; at 20 ℃; for 16h;

DOI:10.1039/c1cc10196j

Reference yield:

dichlorobis(dimethylamino)diborane(4) (64541-76-0) + 4Li(1+)*B2(NC6H5)4(4-)=Li4B2(NC6H5)4 → B2(NPh)4(B2(NMe2)2)2 (1290041-08-5)

Guidance literature:

In not given; Li salt of diborate anion reacted with 2 equiv. of B2Cl2(NMe2)2;

DOI:10.1039/c1cc10196j

upstream raw materials:

dichlorobis(dimethylamino)diborane⁽⁴⁾

tetrakis(phenylamino)diborane⁽⁴⁾