(diethyl acetylenedicarboxylate)bis{(4,4'-dimethyl-2,2'-bipyridine)copper(I)} hexafluoroantimonate

Base Information

Chemical Name:(diethyl acetylenedicarboxylate)bis{(4,4'-dimethyl-2,2'-bipyridine)copper(I)} hexafluoroantimonate
CAS No.:137436-82-9
Molecular Formula:C₃₂H₃₄Cu₂N₄O₄*2F₆Sb
Molecular Weight:1137.22
Hs Code.:

Synonyms:(diethyl acetylenedicarboxylate)bis{(4,4'-dimethyl-2,2'-bipyridine)copper(I)} hexafluoroantimonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (diethyl acetylenedicarboxylate)bis{(4,4'-dimethyl-2,2'-bipyridine)copper(I)} hexafluoroantimonate

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Technology Process of (diethyl acetylenedicarboxylate)bis{(4,4'-dimethyl-2,2'-bipyridine)copper(I)} hexafluoroantimonate

There total 1 articles about (diethyl acetylenedicarboxylate)bis{(4,4'-dimethyl-2,2'-bipyridine)copper(I)} hexafluoroantimonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 137436-75-0
(4,4'-dimethyl-2,2'-bipyridine)(diethyl acetylenedicarboxylate)copper(I) hexafluoroantimonate

: 137436-82-9
(diethyl acetylenedicarboxylate)bis{(4,4'-dimethyl-2,2'-bipyridine)copper(I)} hexafluoroantimonate

: 762-21-0
acetylenedicarboxylic acid diethyl ester

Guidance literature:: In acetone; dissolving of (Cu(Me2bpy)(DEAD))SbF6 in acetone; addn. of hexane, pptn., filtration, two addnl. repptn., washing (hexane, 3 times), drying (vac., overnight); elem. anal.;
DOI:10.1021/om00037a019