3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester

Base Information

Chemical Name:3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester
CAS No.:220965-92-4
Molecular Formula:C₁₈H₂₃N₃O₄
Molecular Weight:345.398
Hs Code.:

Synonyms:3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester

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Chemical Property of 3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester

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Technology Process of 3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester

There total 1 articles about 3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 160842-62-6
3-tert-Butyl-1-methyl-1H-pyrazole-5-carbonyl chloride

: 217314-47-1
methyl 3-amino-5-methoxybenzoate

: 220965-92-4
3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester

Guidance literature:: With pyridine; In dichloromethane; for 17h; Ambient temperature;
DOI:10.1002/jhet.5570350646

Reference yield: 88.0%

: 220965-92-4
3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester

: 220965-93-5
3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid

Guidance literature:: With potassium carbonate; In methanol; for 15h; Ambient temperature;
DOI:10.1002/jhet.5570350646

Reference yield:

: 220965-92-4
3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid, methyl ester

: 3-<<<3-(1,1-dimethylethyl)-1-methyl-1H-pyrazol-5-yl>carbonyl>amino>-5-methoxybenzoic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / aq. K₂CO₃ / methanol / 15 h / Ambient temperature

2: (COCl)2, DMF / CH₂Cl₂ / 3 h / Ambient temperature

With oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In methanol; dichloromethane;
DOI:10.1002/jhet.5570350646