N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine

Base Information

Chemical Name:N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine
CAS No.:1080029-15-7
Molecular Formula:C₂₃H₁₃F₉N₆O
Molecular Weight:560.381
Hs Code.:

Synonyms:N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine

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Chemical Property of N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine

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Technology Process of N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine

There total 3 articles about N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1080029-16-8
N-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamide

: 1080029-15-7
N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine

Guidance literature:: N-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamide; With phosphorus pentoxide; In dichloromethane; toluene; for 20h; Heating / reflux;

With hydroxylamine; In tetrahydrofuran; ethanol; at 0 - 20 ℃; for 20h;

Reference yield:

: 405520-25-4
3-(1 H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-ylamine

: 1080029-15-7
N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 12 h / 20 °C

2.1: phosphorus pentoxide / dichloromethane; toluene / 20 h / Heating / reflux

2.2: 20 h / 0 - 20 °C

With pyridine; phosphorus pentoxide; In dichloromethane; toluene;

Reference yield:

: 785-56-8
3,5-bis(trifluoromethyl)phenyl carboxylic acid chloride

: 1080029-15-7
N-hydroxy-N'-[3-(1H-tetrazol-5-yl)-4'-trifluoromethyl-biphenyl-4-yl]-3,5-bis-trifluoromethyl-benzamidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 12 h / 20 °C

2.1: phosphorus pentoxide / dichloromethane; toluene / 20 h / Heating / reflux

2.2: 20 h / 0 - 20 °C

With pyridine; phosphorus pentoxide; In dichloromethane; toluene;