methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside
CAS No.:1201897-28-0
Molecular Formula:C₅₈H₆₄O₁₁
Molecular Weight:937.14
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside

There total 4 articles about methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 857419-75-1
1-C-acetyl-3,4,6-tri-O-benzyl-1,2-cyclopropane-1,2-deoxy-α-D-glucopyranose

: 1201897-28-0
methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -20 - 20 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo1016579

Reference yield:

: 767340-70-5
1-(3',4',6'-tri-O-benzyl-α-D-mannopyranosyl)prop-2-ene

: 1201897-28-0
methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 20 °C

2: Jones reagent; mercury(II) diacetate / water; acetone / 6 h / 0 °C

3: potassium carbonate / methanol / 20 °C

4: boron trifluoride diethyl etherate / dichloromethane / -20 - 20 °C / Inert atmosphere; Molecular sieve

With pyridine; Jones reagent; boron trifluoride diethyl etherate; mercury(II) diacetate; potassium carbonate; In methanol; dichloromethane; water; acetone;
DOI:10.1021/jo1016579

Reference yield:

: 857419-61-5
3-C-(3',4',6'-tri-O-benzyl-2'-O-tosyl-α-D-mannopyranosyl)-propene

: 1201897-28-0
methyl 2,3,4-tri-O-benzyl-6-O-(3',4',6'-tri-O-benzyl-2'-C-acetylmethyl-2'-deoxy-β-D-galactopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent; mercury(II) diacetate / water; acetone / 6 h / 0 °C

2: potassium carbonate / methanol / 20 °C

3: boron trifluoride diethyl etherate / dichloromethane / -20 - 20 °C / Inert atmosphere; Molecular sieve

With Jones reagent; boron trifluoride diethyl etherate; mercury(II) diacetate; potassium carbonate; In methanol; dichloromethane; water; acetone;
DOI:10.1021/jo1016579