[2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride

Base Information

Chemical Name:[2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride
CAS No.:92269-71-1
Molecular Formula:C₅₁H₆₂N₄O₁₃PS*Cl
Molecular Weight:1037.57
Hs Code.:

[2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride

Synonyms:[2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride

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Chemical Property of [2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride

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Technology Process of [2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride

There total 11 articles about [2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 92269-70-0,121250-44-0
Peoc-3-Cl

: 1849-36-1
para-nitrobenzenethiol

: 92269-71-1
[2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃;

Reference yield:

: 82414-77-5
N-<2-(Triphenylphosphonio)ethoxycarbonyl>valylchlorid-chlorid

: 92269-71-1
[2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride

Guidance literature:: Multi-step reaction with 9 steps

1: 68 percent / pyridine / CH₂Cl₂ / 0 °C

2: 79 percent / dimethylamine / methanol / 0 °C

3: 81 percent / pyridine / CH₂Cl₂ / 0 °C

4: 87 percent / dimethylamine / methanol / 0 °C

5: pyridine / CH₂Cl₂ / 0 °C

6: 85 percent / dimethylamine / methanol / 0 °C

7: 70 percent / pyridine / CH₂Cl₂ / 0 °C

8: 1.) HCl 2.) (COCl)2 / 1.) CH₂Cl₂ 2.) CH₂Cl₂, RT

9: 86 percent / pyridine / CH₂Cl₂ / 0 °C

With pyridine; hydrogenchloride; oxalyl dichloride; dimethyl amine; In methanol; dichloromethane;

Reference yield:

: 92269-65-3
Peoc-Val-Lac-OtBu

: 92269-71-1
[2-((S)-2-Methyl-1-{(S)-1-[(S)-2-methyl-1-((S)-1-{(S)-2-methyl-1-[(S)-1-(4-nitro-phenylsulfanylcarbonyl)-ethoxycarbonyl]-propylcarbamoyl}-ethoxycarbonyl)-propylcarbamoyl]-ethoxycarbonyl}-propylcarbamoyloxy)-ethyl]-triphenyl-phosphonium; chloride

Guidance literature:: Multi-step reaction with 8 steps

1: 79 percent / dimethylamine / methanol / 0 °C

2: 81 percent / pyridine / CH₂Cl₂ / 0 °C

3: 87 percent / dimethylamine / methanol / 0 °C

4: pyridine / CH₂Cl₂ / 0 °C

5: 85 percent / dimethylamine / methanol / 0 °C

6: 70 percent / pyridine / CH₂Cl₂ / 0 °C

7: 1.) HCl 2.) (COCl)2 / 1.) CH₂Cl₂ 2.) CH₂Cl₂, RT

8: 86 percent / pyridine / CH₂Cl₂ / 0 °C

With pyridine; hydrogenchloride; oxalyl dichloride; dimethyl amine; In methanol; dichloromethane;