cis-2,2'-difluoro-α,α'-epoxy bibenzyl

Base Information

• Chemical Name: cis-2,2'-difluoro-α,α'-epoxy bibenzyl
• CAS No.: 13528-40-0
• Molecular Formula: C₁₄H₁₀F₂O
• Molecular Weight: 232.23

Synonyms:cis-2,2'-difluoro-α,α'-epoxy bibenzyl

Chemical Property of cis-2,2'-difluoro-α,α'-epoxy bibenzyl

Chemical Property:

Purity/Quality:

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Technology Process of cis-2,2'-difluoro-α,α'-epoxy bibenzyl

There total 2 articles about cis-2,2'-difluoro-α,α'-epoxy bibenzyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Fluorobenzaldehyde (446-52-6) → cis-2,2'-difluoro-α,α'-epoxy bibenzyl (13528-40-0)

Guidance literature:

With hexaethylphosphoric triamide; In hexane; benzene; at 20 ℃; for 24h;

DOI:10.1021/ja0466210

Reference yield:

→ cis-2,2'-difluoro-α,α'-epoxy bibenzyl (13528-40-0)

Guidance literature:

2-Fluorbenzaldehyd (2Mol), (Me2N)3P (1Mol); neben dem trans-Isomeren;

DOI:10.1021/ja00895a051

Reference yield:

cis-2,2'-difluoro-α,α'-epoxy bibenzyl (13528-40-0) → (S,S)-1,2-bis(2-fluorophenyl)-1,2-ethanediol + (R,R)-1,2-bis(2-fluorophenyl)-1,2-ethanediol

Guidance literature:

With BD₈₈₇₇; In phosphate buffer; acetonitrile; at 22 ℃; pH=7.5; Title compound not separated from byproducts;

DOI:10.1021/ja0466210

upstream raw materials:

2-Fluorobenzaldehyde

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