4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione

Base Information

• Chemical Name: 4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione
• CAS No.: 114133-18-5
• Molecular Formula: C₂₉H₂₄N₂O₆
• Molecular Weight: 496.519

Synonyms:4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione

Chemical Property of 4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione

Chemical Property:

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Technology Process of 4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione

There total 3 articles about 4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-phenyl-maleimide (941-69-5) + 1-(benzoyloxy)-5-(carbaniloyloxy)-1(E),3(E)-pentadiene (114132-99-9) → 4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione (114133-18-5)

Guidance literature:

With 2,6-di-tert-butyl-4-methyl-phenol; In chloroform; for 120h; Heating;

DOI:10.1021/jo00244a005

Reference yield:

1-(benzoyloxy)-5-hydroxy-1(E),3(E)-pentadiene (40418-53-9) → 4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione (114133-18-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 42 percent / toluene / 1.5 h / Heating

2: 70 percent / 2,6-di-tert-butyl-p-cresol / CHCl₃ / 120 h / Heating

With 2,6-di-tert-butyl-4-methyl-phenol; In chloroform; toluene;

DOI:10.1021/jo00244a005

Reference yield:

phenyl isocyanate (103-71-9) → 4-<(carbaniloyloxy)methyl>-7-(benzoyloxy)-3a,4,7,7a-tetrahydro-2-phenyl-1,3-isoindoledione (114133-18-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 42 percent / toluene / 1.5 h / Heating

2: 70 percent / 2,6-di-tert-butyl-p-cresol / CHCl₃ / 120 h / Heating

With 2,6-di-tert-butyl-4-methyl-phenol; In chloroform; toluene;

DOI:10.1021/jo00244a005

upstream raw materials:

N-phenyl-maleimide

1-(benzoyloxy)-5-(carbaniloyloxy)-1(E),3(E)-pentadiene

1-(benzoyloxy)-5-hydroxy-1(E),3(E)-pentadiene

phenyl isocyanate

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