1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester

Base Information

Chemical Name:1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester
CAS No.:309920-58-9
Molecular Formula:C₂₇H₂₀F₅NO₄
Molecular Weight:517.452
Hs Code.:

Synonyms:1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester

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Chemical Property of 1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester

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Technology Process of 1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester

There total 3 articles about 1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 117322-30-2
1-<(fluorenylmethyloxycarbonyl)amino>cyclopentane-1-carboxylic acid

: 309920-58-9
1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; at 0 - 20 ℃; for 14h;
DOI:10.1021/ja0019225

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 309920-58-9
1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / NaHCO₃ / H₂O; acetone / 12 h

2: 64 percent / dicyclohexylcarbodiimide / ethyl acetate / 14 h / 0 - 20 °C

With sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In water; ethyl acetate; acetone;
DOI:10.1021/ja0019225

Reference yield:

: 52-52-8
1-amino-1-cyclopentanecarboxylic acid

: 309920-58-9
1-(9H-fluoren-9-ylmethoxycarbonylamino)-cyclopentanecarboxylic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / NaHCO₃ / H₂O; acetone / 12 h

2: 64 percent / dicyclohexylcarbodiimide / ethyl acetate / 14 h / 0 - 20 °C

With sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In water; ethyl acetate; acetone;
DOI:10.1021/ja0019225