Technology Process of C17H11(2)H4N5O3
There total 3 articles about C17H11(2)H4N5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; potassium tert-butylate;
In
dimethyl sulfoxide;
at 20 ℃;
for 24h;
DOI:10.1002/jlcr.817
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 61 percent / potassium acetate; tetrakis(triphenylphosphine)-palladium(0) / dimethylformamide / 120 °C
2: 94 percent / hydroxylamine hydrochloride; potassium t-butoxide / dimethylsulfoxide / 24 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); hydroxylamine hydrochloride; potassium tert-butylate; potassium acetate;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
1: Heck reaction;
DOI:10.1002/jlcr.817
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 54 percent / dimethylformamide / 24 h / 110 - 120 °C
2: 61 percent / potassium acetate; tetrakis(triphenylphosphine)-palladium(0) / dimethylformamide / 120 °C
3: 94 percent / hydroxylamine hydrochloride; potassium t-butoxide / dimethylsulfoxide / 24 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); hydroxylamine hydrochloride; potassium tert-butylate; potassium acetate;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
2: Heck reaction;
DOI:10.1002/jlcr.817