[(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester

Base Information

Chemical Name:[(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester
CAS No.:78827-79-9
Molecular Formula:C₁₄H₁₈N₂O₄
Molecular Weight:278.308
Hs Code.:

Synonyms:[(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester

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Chemical Property of [(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of [(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester

There total 4 articles about [(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 78827-74-4
7-Methoxy-2-methyl-benzo[d][1,3]diazepine-3-carboxylic acid ethyl ester

: 78827-79-9
[(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester

Guidance literature:: With hydrogenchloride; In methanol; for 2h; Ambient temperature;
DOI:10.1248/cpb.30.3757

Reference yield:

: 78827-69-7
C₁₄H₁₆N₂O₃

: 78827-79-9
[(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Irradiation

2: 10percent aq. HCl / Ambient temperature

With hydrogenchloride;
DOI:10.1039/c39810000211

Reference yield:

: 1078-28-0
6-methoxyquinaldine

: 78827-79-9
[(Z)-2-(2-Acetylamino-5-methoxy-phenyl)-vinyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / CH₂Cl₂ / 1 h / Ambient temperature

2: 61 percent / potassium carbonate / ethanol / 8 h / Ambient temperature

3: 48 percent / benzene / Irradiation

4: 63 percent / 10 percent HCl / methanol / 2 h / Ambient temperature

With hydrogenchloride; potassium carbonate; In methanol; ethanol; dichloromethane; benzene;
DOI:10.1248/cpb.30.3757