7,8-dimethoxy-3-(4-(tert-butoxycarbonylaminomethyl)anilinocarbonyl)-1H-pyrrolo[3,2-c]quinoline

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Chemical Name:7,8-dimethoxy-3-(4-(tert-butoxycarbonylaminomethyl)anilinocarbonyl)-1H-pyrrolo[3,2-c]quinoline
CAS No.:358680-96-3
Molecular Formula:C₂₆H₂₈N₄O₅
Molecular Weight:476.532
Hs Code.:

Synonyms:7,8-dimethoxy-3-(4-(tert-butoxycarbonylaminomethyl)anilinocarbonyl)-1H-pyrrolo[3,2-c]quinoline

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Chemical Property of 7,8-dimethoxy-3-(4-(tert-butoxycarbonylaminomethyl)anilinocarbonyl)-1H-pyrrolo[3,2-c]quinoline

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Technology Process of 7,8-dimethoxy-3-(4-(tert-butoxycarbonylaminomethyl)anilinocarbonyl)-1H-pyrrolo[3,2-c]quinoline

There total 2 articles about 7,8-dimethoxy-3-(4-(tert-butoxycarbonylaminomethyl)anilinocarbonyl)-1H-pyrrolo[3,2-c]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 94838-55-8
tert-butyl (4-aminobenzyl)carbamate

: 358680-95-2
7,8-dimethoxy-1H-pyrrolo[3,2-c]quinoline-3-carboxylic acid

: 358680-96-3
7,8-dimethoxy-3-(4-(tert-butoxycarbonylaminomethyl)anilinocarbonyl)-1H-pyrrolo[3,2-c]quinoline

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1002/jhet.5570380335

Reference yield:

: 358680-94-1
ethyl 7,8-dimethoxy-1H-pyrrolo[3,2-c]quinoline-3-carboxylate

: 358680-96-3
7,8-dimethoxy-3-(4-(tert-butoxycarbonylaminomethyl)anilinocarbonyl)-1H-pyrrolo[3,2-c]quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / 10 percent aq. NaOH / methanol / 18 h / 20 °C

2: 28 percent / PyBOP; DIPEA / dimethylformamide / 24 h / 20 °C

With sodium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570380335