C₁₈H₁₇BrIN₃OS

Base Information

Chemical Name:C₁₈H₁₇BrIN₃OS
CAS No.:1404488-82-9
Molecular Formula:C₁₈H₁₇BrIN₃OS
Molecular Weight:530.227
Hs Code.:

C<sub>18</sub>H<sub>17</sub>BrIN<sub>3</sub>OS

Synonyms:C₁₈H₁₇BrIN₃OS

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Chemical Property of C₁₈H₁₇BrIN₃OS

Chemical Property:

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Technology Process of C₁₈H₁₇BrIN₃OS

There total 5 articles about C₁₈H₁₇BrIN₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1404488-81-8
C₁₀H₁₃BrN₂

: 532-55-8
Benzoyl isothiocyanate

: 1404488-82-9
C₁₈H₁₇BrIN₃OS

Guidance literature:: C₁₀H₁₃BrN₂; Benzoyl isothiocyanate; In dichloromethane; at 0 ℃; for 0.333333h;

With iodine; toluene-4-sulfonic acid; In acetonitrile; at 20 ℃; for 2h; Cooling with ice;

Reference yield:

: 1612761-56-4
C₁₁H₁₅BrN₂OS

: 1404488-82-9
C₁₈H₁₇BrIN₃OS

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran; diethyl ether / 0.5 h / -70 °C

2.1: hydrogenchloride / methanol / 0.33 h / 20 °C

3.1: dichloromethane / 0.33 h / 0 °C

3.2: 2 h / 20 °C / Cooling with ice

With hydrogenchloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;

Reference yield:

: 1060805-69-7
1-(4-bromopyridin-2-yl)ethan-1-one

: 1404488-82-9
C₁₈H₁₇BrIN₃OS

Guidance literature:: Multi-step reaction with 4 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 3 h / Inert atmosphere; Reflux

2.1: tetrahydrofuran; diethyl ether / 0.5 h / -70 °C

3.1: hydrogenchloride / methanol / 0.33 h / 20 °C

4.1: dichloromethane / 0.33 h / 0 °C

4.2: 2 h / 20 °C / Cooling with ice

With hydrogenchloride; titanium(IV) tetraethanolate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;