hexyl(4-(trifluoromethyl)phenyl)sulfane

Base Information

• Chemical Name: hexyl(4-(trifluoromethyl)phenyl)sulfane
• CAS No.: 1446428-08-5
• Molecular Formula: C₁₃H₁₇F₃S
• Molecular Weight: 262.339
• Mol file: 1446428-08-5.mol

Synonyms:hexyl(4-(trifluoromethyl)phenyl)sulfane

Chemical Property of hexyl(4-(trifluoromethyl)phenyl)sulfane

Chemical Property:

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Technology Process of hexyl(4-(trifluoromethyl)phenyl)sulfane

There total 1 articles about hexyl(4-(trifluoromethyl)phenyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

4-(hexylthio)aniline (16098-23-0) + trifluoromethylsilver → hexyl(4-(trifluoromethyl)phenyl)sulfane (1446428-08-5)

Guidance literature:

4-(hexylthio)aniline; With hydrogenchloride; In water; at 0 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

With tert.-butylnitrite; at 0 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

trifluoromethylsilver; at -78 - 20 ℃; for 4h; Inert atmosphere; Schlenk technique;

DOI:10.1021/ja4056239

upstream raw materials:

4-(hexylthio)aniline