3,4-methylenedioxy-5.4'-dimethoxy-3'-(O^β-tert-butyl-N^α-Boc-L-Asp)-amido-Z-stilbene

Base Information

• Chemical Name: 3,4-methylenedioxy-5.4'-dimethoxy-3'-(O^β-tert-butyl-N^α-Boc-L-Asp)-amido-Z-stilbene
• CAS No.: 865717-78-8
• Molecular Formula: C₃₀H₃₈N₂O₉
• Molecular Weight: 570.64

Synonyms:3,4-methylenedioxy-5.4'-dimethoxy-3'-(O^β-tert-butyl-N^α-Boc-L-Asp)-amido-Z-stilbene

Chemical Property of 3,4-methylenedioxy-5.4'-dimethoxy-3'-(O^β-tert-butyl-N^α-Boc-L-Asp)-amido-Z-stilbene

Chemical Property:

Purity/Quality:

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Technology Process of 3,4-methylenedioxy-5.4'-dimethoxy-3'-(O^β-tert-butyl-N^α-Boc-L-Asp)-amido-Z-stilbene

There total 1 articles about 3,4-methylenedioxy-5.4'-dimethoxy-3'-(O^β-tert-butyl-N^α-Boc-L-Asp)-amido-Z-stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

Boc-Asp(OtBu)-OH (1676-90-0) + 2-Methoxy-5-[(Z)-2-(7-methoxy-benzo[1,3]dioxol-5-yl)-vinyl]-phenylamine (501033-98-3) → 3,4-methylenedioxy-5.4'-dimethoxy-3'-(Oβ-tert-butyl-Nα-Boc-L-Asp)-amido-Z-stilbene (865717-78-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 1.25h;

DOI:10.1021/np058033l

Reference yield:

3,4-methylenedioxy-5.4'-dimethoxy-3'-(Oβ-tert-butyl-Nα-Boc-L-Asp)-amido-Z-stilbene (865717-78-8) → C2HF3O2*C21H22N2O7

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; for 4h;

Reference yield:

3,4-methylenedioxy-5.4'-dimethoxy-3'-(Oβ-tert-butyl-Nα-Boc-L-Asp)-amido-Z-stilbene (865717-78-8) + trifluoroacetic acid (76-05-1) → C2HF3O2*C21H22N2O7

Guidance literature:

With triethylsilane; In dichloromethane; for 4h;

DOI:10.1021/np058033l

upstream raw materials:

Boc-Asp(OtBu)-OH

2-Methoxy-5-[(Z)-2-(7-methoxy-benzo[1,3]dioxol-5-yl)-vinyl]-phenylamine

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