5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene

Base Information

• Chemical Name: 5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene
• CAS No.: 910112-06-0
• Molecular Formula: C₃₆H₃₂N₂O₂S
• Molecular Weight: 556.728

Synonyms:5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene

Chemical Property of 5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene

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Technology Process of 5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene

There total 4 articles about 5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

12-pentyl-5-p-tosyl-5,11-dihydroindolo[3,2-b]carbazole (910112-01-5) + iodobenzene (591-50-4) → 5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene (910112-06-0)

Guidance literature:

With copper; In 1,2-dichloro-benzene; at 190 ℃;

DOI:10.1055/s-2006-944183

Reference yield:

12-pentyl-5,11-dihydroindolo[3,2-b]carbazole (910111-97-6) → 5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene (910112-06-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / NaH / dimethylformamide / -20 - 70 °C

2: 70 percent / K₂CO₃; copper bronze / 1,2-dichloro-benzene / 190 °C

With copper; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; 1,2-dichloro-benzene; 2: Ullmann coupling;

DOI:10.1021/jo0711337

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → 5-pentyl-6-phenyl-12-(toluene-4-sulfonyl)-6,12-dihydro-6,12-diaza-indeno[1,2-b]fluorene (910112-06-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / NaH / dimethylformamide / -20 - 70 °C

2: 70 percent / K₂CO₃; copper bronze / 1,2-dichloro-benzene / 190 °C

With copper; sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; 1,2-dichloro-benzene; 2: Ullmann coupling;

DOI:10.1021/jo0711337

upstream raw materials:

12-pentyl-5-p-tosyl-5,11-dihydroindolo[3,2-b]carbazole

iodobenzene

12-pentyl-5,11-dihydroindolo[3,2-b]carbazole

p-toluenesulfonyl chloride

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