2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine

Base Information

Chemical Name:2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine
CAS No.:933069-17-1
Molecular Formula:C₃₈H₃₂N₄O₈
Molecular Weight:672.694
Hs Code.:

Synonyms:2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine

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Chemical Property of 2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine

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Technology Process of 2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine

There total 3 articles about 2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 917235-49-5
2-(benzoyloxymethyl)-6-chloro-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-furanosyl)purine

: 13331-23-2
fur-2-ylboronic acid

: 933069-17-1
2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 100 ℃; for 12h;
DOI:10.1135/cccc20060788

Reference yield:

: 118706-48-2
6-chloro-2-iodo-9-[2’-deoxy-3’,5’-di-O-(4-methylbenzoyl)-β-D-ribofuranosyl]purine

: 933069-17-1
2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(PPh₃)4 / tetrahydrofuran / 8 h / 20 °C

2: 71 percent / K₂CO₃ / Pd(PPh₃)4 / dimethylformamide / 12 h / 100 °C

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide; 2: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1135/cccc20060788

Reference yield:

: 14135-39-8
[(benzoyloxy)methyl]zinc iodide

: 933069-17-1
2-[(benzoyloxy)methyl]-6-(2-furyl)-9-(2-deoxy-3,5-di-O-p-toluoyl-β-D-erythro-pentofuranosyl)purine

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(PPh₃)4 / tetrahydrofuran / 8 h / 20 °C

2: 71 percent / K₂CO₃ / Pd(PPh₃)4 / dimethylformamide / 12 h / 100 °C

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide; 2: Suzuki-Miyaura cross-coupling reaction;
DOI:10.1135/cccc20060788