1,2,2-Trimethyl-3-(4-(methylthio)benzoyl)cyclopentanecarboxylic acid

Base Information

Chemical Name:1,2,2-Trimethyl-3-(4-(methylthio)benzoyl)cyclopentanecarboxylic acid
CAS No.:61469-03-2
Molecular Formula:C17H22O3S
Molecular Weight:306.4198
Hs Code.:
Mol file:61469-03-2.mol

Synonyms:3-thioanisoyl-1,2,2-trimethylcyclopentane-1-carboxylic acid;3-TTCCA;p-3-thioanisoyl-1,2,2-trimethylcyclopentane-1-carboxylic acid

Suppliers and Price of 1,2,2-Trimethyl-3-(4-(methylthio)benzoyl)cyclopentanecarboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,2,2-Trimethyl-3-(4-(methylthio)benzoyl)cyclopentanecarboxylic acid

Chemical Property:

Vapor Pressure:1.9E-09mmHg at 25°C
Boiling Point:465°Cat760mmHg
Flash Point:235°C
PSA：79.67000
Density:1.18g/cm³
LogP:4.11830
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:306.12896573
Heavy Atom Count:21
Complexity:424

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(CCC1(C)C(=O)O)C(=O)C2=CC=C(C=C2)SC)C

Technology Process of 1,2,2-Trimethyl-3-(4-(methylthio)benzoyl)cyclopentanecarboxylic acid

There total 1 articles about 1,2,2-Trimethyl-3-(4-(methylthio)benzoyl)cyclopentanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61469-03-2
1,2,2-Trimethyl-3-(4-methylsulfanyl-benzoyl)-cyclopentanecarboxylic acid

Guidance literature:: Camphersaeureanhydrid, Thioanisol, AlCl3;

Reference yield:

: 61469-03-2,104225-31-2,122082-19-3,145918-70-3
(1R,3S)-1,2,2-Trimethyl-3-(4-methylsulfanyl-benzoyl)-cyclopentanecarboxylic acid

: 122082-52-4
(1R,6S)-1,9,9-Trimethyl-5-(4-methylsulfanyl-phenyl)-3-oxa-4-aza-bicyclo[4.2.1]nonane; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: 87 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

3: 1.) LiAlH₄; 2.) HCl gas / 1.) ether, reflux, 24 h; 2.) ether

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; hydroxylamine hydrochloride; In diethyl ether; ethanol;
DOI:10.1016/0223-5234(88)90091-8

Reference yield:

: 61469-03-2,104225-31-2,122082-19-3,145918-70-3
(1R,3S)-1,2,2-Trimethyl-3-(4-methylsulfanyl-benzoyl)-cyclopentanecarboxylic acid

: 122082-40-0
(1S,3R)-3-[[(E)-Hydroxyimino]-(4-methylsulfanyl-phenyl)-methyl]-1,2,2-trimethyl-cyclopentanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: 87 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

With pyridine; hydroxylamine hydrochloride; In diethyl ether; ethanol;
DOI:10.1016/0223-5234(88)90091-8