2,5-diiodo-4-octyloxyphenol

Base Information

• Chemical Name: 2,5-diiodo-4-octyloxyphenol
• CAS No.: 911307-60-3
• Molecular Formula: C₁₄H₂₀I₂O₂
• Molecular Weight: 474.121
• Mol file: 911307-60-3.mol

Synonyms:2,5-diiodo-4-octyloxyphenol

Chemical Property of 2,5-diiodo-4-octyloxyphenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-diiodo-4-octyloxyphenol

There total 5 articles about 2,5-diiodo-4-octyloxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

1,4-diiodo-2,5-dioctyloxybenzene (145483-68-7) → 2,5-diiodo-4-octyloxyphenol (911307-60-3)

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.08.132

Reference yield: 56.0%

1-bromo-octane (111-83-1) + 2,5-diiodo-1,4-hydroquinone (13064-64-7) → 2,5-diiodo-4-octyloxyphenol (911307-60-3)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 20h;

DOI:10.1039/b208190c

Reference yield: 28.0%

1-bromo-octane (111-83-1) + 2,5-diiodo-1,4-hydroquinone (13064-64-7) → 1,4-diiodo-2,5-dioctyloxybenzene (145483-68-7) + 2,5-diiodo-4-octyloxyphenol (911307-60-3)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; acetone; for 24h; Reflux; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.tetlet.2012.08.132

upstream raw materials:

1-bromo-octane

2,5-diiodo-1,4-hydroquinone

1,4-diiodo-2,5-dimethoxybenzene

1,4-diiodo-2,5-dioctyloxybenzene

Refernces

• 1、 Zhang, Junxiang,Cui, Yiping,Wang, Mingliang,Liu, Juzheng. "Synthesis of double-conjugated-segment molecules and their application as ultra-broad two-photon-absorption optical limiters". . p. 2526 - 2527. Retrieved 2007/10/03.