C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-)

Base Information

Chemical Name:C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-)
CAS No.:1352917-01-1
Molecular Formula:C₂₁H₂₈ClN₂*Cl
Molecular Weight:379.373
Hs Code.:

C<sub>21</sub>H<sub>28</sub>ClN<sub>2</sub><sup>(1+)</sup>*Cl<sup>(1-)</sup>

Synonyms:C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-)

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Chemical Property of C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-)

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Technology Process of C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-)

There total 4 articles about C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1352916-98-3
C₂₀H₂₉ClN₂

: 122-51-0
orthoformic acid triethyl ester

: 1352917-01-1
C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-)

Guidance literature:: C₂₀H₂₉ClN₂; With hydrogenchloride; In diethyl ether; Inert atmosphere;

orthoformic acid triethyl ester; at 120 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja3119288

Reference yield:

: 24596-18-7
4-chloro-2,6-dimethylaniline

: 1352917-01-1
C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 25 °C / Inert atmosphere

2.1: potassium carbonate / acetonitrile / 16 h / 85 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 36 h / 0 - 65 °C / Inert atmosphere

4.1: hydrogenchloride / diethyl ether / Inert atmosphere

4.2: 0.5 h / 120 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1021/ja3119288

Reference yield:

: 2-bromo-N-(4-chloro-2,6-dimethylphenyl)acetamide

: 1352917-01-1
C₂₁H₂₈ClN₂⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 16 h / 85 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 36 h / 0 - 65 °C / Inert atmosphere

3.1: hydrogenchloride / diethyl ether / Inert atmosphere

3.2: 0.5 h / 120 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1021/ja3119288