p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside
CAS No.:14419-60-4
Molecular Formula:C₂₂H₂₈N₂O₁₀
Molecular Weight:480.472
Hs Code.:

Synonyms:p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside

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Technology Process of p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside

There total 6 articles about p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 65907-85-9
p-aminophenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-O-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: 14419-60-4
p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside

Guidance literature:: With pyridine; for 1h; Ambient temperature;

Reference yield:

: 103-90-2,8055-08-1
4-acetaminophenol

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 14419-60-4
p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; at 20 ℃;
DOI:10.1021/ja0567687

Reference yield:

: 13089-27-5,13089-23-1
p-nitrophenyl 2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranoside

: 14419-60-4
p-N-acetamidophenyl 2-acetamido-3,4,6-tri-O-acety-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / ammonium formate / 10percent Pd/C / methanol / 0.03 h / Heating

2: 96 percent / pyridine / 1 h / Ambient temperature

With pyridine; ammonium formate; palladium on activated charcoal; In methanol;