Technology Process of C28H34N2O3
There total 6 articles about C28H34N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: SOCl2 / DMF / ethyl acetate / 6 h / 20 - 50 °C
2: aq. NaHCO3 / ethyl acetate / 1 h / 20 °C
3: HCO2NH4 / Pd/C / methanol / 50 °C
With
thionyl chloride; ammonium formate; sodium hydrogencarbonate;
palladium on activated charcoal; N,N-dimethyl-formamide;
In
methanol; ethyl acetate;
DOI:10.1021/jm070284z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aq. NaHCO3 / ethyl acetate / 1 h / 20 °C
2: HCO2NH4 / Pd/C / methanol / 50 °C
With
ammonium formate; sodium hydrogencarbonate;
palladium on activated charcoal;
In
methanol; ethyl acetate;
DOI:10.1021/jm070284z
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium tetrahydroborate; methanesulfonic acid / diethylene glycol dimethyl ether; isopropyl alcohol / 12 h / 0 - 5 °C
1.2: 0.5 h / 0 - 5 °C
1.3: 3 h / 15 °C
2.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 4 h / 20 °C
3.1: ammonium formate; palladium 10% on activated carbon / methanol / 15 h / 50 °C
With
sodium tetrahydroborate; methanesulfonic acid; palladium 10% on activated carbon; ammonium formate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
methanol; diethylene glycol dimethyl ether; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/acs.jmedchem.0c00529