5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene

Base Information

Chemical Name:5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene
CAS No.:1426414-37-0
Molecular Formula:C₅₆H₄₀O₂
Molecular Weight:744.932
Hs Code.:

Synonyms:5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene

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Chemical Property of 5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene

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Technology Process of 5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene

There total 1 articles about 5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1426414-32-5
5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-6,11-ethanonaphthacene-cis-13,14-diyl carbonate

: 1426414-37-0
5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; water; for 2h; Reflux; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.01.014

Reference yield: 82.0%

: 1426414-37-0
5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene

: 1426414-19-8
5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-6,11-ethanonaphthacene-13,14-dione

Guidance literature:: 5,12-di([1,1':3',1''-terphenyl]-5'-yl)-6,11-dihydro-13,14-dihydroxy-6,11-ethanonaphtacene; With dimethyl sulfoxide; trifluoroacetic anhydride; In dichloromethane; at -60 ℃; for 1.5h; Inert atmosphere;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -60 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.01.014