1-phenyl-3,4-dimethylphosphole selenide

Base Information

• Chemical Name: 1-phenyl-3,4-dimethylphosphole selenide
• CAS No.: 38066-23-8
• Molecular Formula: C₁₂H₁₃PSe
• Molecular Weight: 267.169
• Mol file: 38066-23-8.mol

Synonyms:1-phenyl-3,4-dimethylphosphole selenide

Chemical Property of 1-phenyl-3,4-dimethylphosphole selenide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-phenyl-3,4-dimethylphosphole selenide

There total 2 articles about 1-phenyl-3,4-dimethylphosphole selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dimethyl-1-phenylphosphole (30540-36-4) → 1-phenyl-3,4-dimethylphosphole selenide (38066-23-8)

Guidance literature:

With selenium; In benzene; Heating;

DOI:10.1016/S0040-4020(01)93648-8

Reference yield:

selenium (7782-49-2) + 3,4-dimethyl-1-phenylphosphole (30540-36-4) → 1-phenyl-3,4-dimethylphosphole selenide (38066-23-8)

Guidance literature:

In chloroform-d1; at 0 ℃; for 24h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om301244m

Reference yield: 79.0%

C22H15NSe (864182-15-0) + 1-phenyl-3,4-dimethylphosphole selenide (38066-23-8) → C20H18NPSe2

Guidance literature:

In toluene; for 4h; Heating;

DOI:10.1016/j.tetlet.2007.03.079

upstream raw materials:

3,4-dimethyl-1-phenylphosphole

selenium

Downstream raw materials:

4-Phenylurazole

(1R,2R,6R,7S,10R)-5,6,8,9-Tetramethyl-3,10-diphenyl-3,10-diphospha-tricyclo[5.2.1.0^2,6]deca-4,8-diene 3,10-dioxide

phenyl-selenophosphonsaeure-dimethylester

phenyl-selenophosphonigsaeure-methylester

Refernces