C₂₂H₁₉ClN₂

Base Information

Chemical Name:C₂₂H₁₉ClN₂
CAS No.:1283086-63-4
Molecular Formula:C₂₂H₁₉ClN₂
Molecular Weight:346.859
Hs Code.:

C<sub>22</sub>H<sub>19</sub>ClN<sub>2</sub>

Synonyms:C₂₂H₁₉ClN₂

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Chemical Property of C₂₂H₁₉ClN₂

Chemical Property:

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Technology Process of C₂₂H₁₉ClN₂

There total 4 articles about C₂₂H₁₉ClN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1283086-87-2
7-methyl-3,4,5,10-tetrahydro-1H-2,5-methanoazepino[3,4-b]indole

: 33491-03-1
1-(bromoethynyl)-4-chlorobenzene

: 1283086-63-4
C₂₂H₁₉ClN₂

Guidance literature:: With potassium phosphate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; In toluene; at 80 ℃; for 16h; Inert atmosphere;

Reference yield:

: 614-96-0
5-methyl-1H-indole

: 1283086-63-4
C₂₂H₁₉ClN₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / 24 h / 90 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Reflux

3.1: trifluoroacetic acid / ethanol / 3 h / Reflux

3.2: 2 h / Reflux

4.1: potassium phosphate; 1,10-Phenanthroline / copper(ll) sulfate pentahydrate / toluene / 16 h / 80 °C / Inert atmosphere

With potassium phosphate; lithium aluminium tetrahydride; 1,10-Phenanthroline; acetic acid; trifluoroacetic acid; copper(ll) sulfate pentahydrate; In tetrahydrofuran; ethanol; toluene; 3.1: Pictet-Spengler Cyclisation / 3.2: Pictet-Spengler Cyclisation;

Reference yield:

: 1283086-86-1
5-methyl-3-(pyrrolidin-3-yl)-1H-indole

: 1283086-63-4
C₂₂H₁₉ClN₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / ethanol / 3 h / Reflux

1.2: 2 h / Reflux

2.1: potassium phosphate; 1,10-Phenanthroline / copper(ll) sulfate pentahydrate / toluene / 16 h / 80 °C / Inert atmosphere

With potassium phosphate; 1,10-Phenanthroline; trifluoroacetic acid; copper(ll) sulfate pentahydrate; In ethanol; toluene; 1.1: Pictet-Spengler Cyclisation / 1.2: Pictet-Spengler Cyclisation;