(E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide

Base Information

Chemical Name:(E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide
CAS No.:1551274-40-8
Molecular Formula:C₁₇H₁₅INS*I
Molecular Weight:519.188
Hs Code.:

Synonyms:(E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide

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Chemical Property of (E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide

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Technology Process of (E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide

There total 5 articles about (E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1551274-27-1
N,N-dimethyl-2-(phenylethynyl)benzothioamide

: 1551274-40-8
(E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide

Guidance literature:: With iodine; In chloroform; at 20 ℃; for 48h; Solvent; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.12.094

Reference yield:

: 54616-46-5
2-Iodo-N,N-dimethylbenzamide

: 1551274-40-8
(E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 48 h / 50 °C / Inert atmosphere

2: Lawessons reagent / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere

3: iodine / chloroform / 48 h / 20 °C / Inert atmosphere

With Lawessons reagent; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; triethylamine; In tetrahydrofuran; chloroform;
DOI:10.1016/j.tetlet.2013.12.094

Reference yield:

: 88-67-5
2-Iodobenzoic acid

: 1551274-40-8
(E)-N-(3-(iodo(phenyl)methylene)benzo[c]thiophen-1(3H)-ylidene)-N-methylmethanaminium iodide

Guidance literature:: Multi-step reaction with 4 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 96 h / 0 - 20 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / 48 h / 50 °C / Inert atmosphere

3: Lawessons reagent / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere

4: iodine / chloroform / 48 h / 20 °C / Inert atmosphere

With Lawessons reagent; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; chloroform;
DOI:10.1016/j.tetlet.2013.12.094