benzyl benzyl(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate

Base Information

• Chemical Name: benzyl benzyl(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate
• CAS No.: 1447701-18-9
• Molecular Formula: C₇₃H₈₁Cl₃N₂O₁₆
• Molecular Weight: 1348.81

Synonyms:benzyl benzyl(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate

Chemical Property of benzyl benzyl(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate

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Technology Process of benzyl benzyl(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate

There total 1 articles about benzyl benzyl(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

benzyl N-benzyl-N-(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate (1447700-80-2) + C33H36Cl3NO8S (1447701-17-8) → benzyl benzyl(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate (1447701-18-9)

Guidance literature:

benzyl N-benzyl-N-(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate; C₃₃H₃₆Cl₃NO₈S; In dichloromethane; at 25 ℃; for 2h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -20 ℃; for 2h; Molecular sieve; Inert atmosphere;

DOI:10.1021/ja403609x

Reference yield: 66.0%

benzyl benzyl(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate (1447701-18-9) → ((2R,3S,4R,5R,6S)-6-((2R,3R,4S,5S,6R)-2-(5-(benzyl(benzyloxycarbonyl)amino)pS33entyloxy)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-4-yloxy)-3-(benzyloxy)-4-hydroxy-5-((2,2,2-trichloroethoxy)carbonylamino)tetrahydro-2H-pyran-2-yl)methyl acetate (1447700-94-8)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 25 ℃; for 2h;

DOI:10.1021/ja403609x

upstream raw materials:

benzyl N-benzyl-N-(5-((2R,3R,4S,5R,6R)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)-4-hydroxytetrahydro-2H-pyran-2-yloxy)pentyl)carbamate

C₃₃H₃₆Cl₃NO₈S

Downstream raw materials:

((2R,3S,4R,5R,6S)-6-((2R,3R,4S,5S,6R)-2-(5-(benzyl(benzyloxycarbonyl)amino)pS₃₃entyloxy)-3,5-bis(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-4-yloxy)-3-(benzyloxy)-4-hydroxy-5-((2,2,2-trichloroethoxy)carbonylamino)tetrahydro-2H-pyran-2-yl)methyl acetate

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