C₂₂H₂₅N₉OSi

Base Information

• Chemical Name: C₂₂H₂₅N₉OSi
• CAS No.: 1338693-28-9
• Molecular Formula: C₂₂H₂₅N₉OSi
• Molecular Weight: 459.586
• Mol file: 1338693-28-9.mol

Synonyms:C₂₂H₂₅N₉OSi

Chemical Property of C₂₂H₂₅N₉OSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₅N₉OSi

There total 3 articles about C₂₂H₂₅N₉OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C22H25Cl2N3OSi (1338693-22-3) → C22H25N9OSi (1338693-28-9)

Guidance literature:

With trimethylsilylazide; In acetonitrile; at 20 ℃; for 17h; Inert atmosphere;

DOI:10.1039/c1dt10898k

Reference yield:

lithium N,N’-diisopropyl-benzamidinate → C22H25N9OSi (1338693-28-9)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrachlorosilane / diethyl ether / 4 h / -78 - 20 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere

3: trimethylsilylazide / acetonitrile / 17 h / 20 °C / Inert atmosphere

With tetrachlorosilane; trimethylsilylazide; triethylamine; In tetrahydrofuran; diethyl ether; acetonitrile;

DOI:10.1039/c1dt10898k

Reference yield:

C13H19Cl3N2Si (1338693-20-1) → C22H25N9OSi (1338693-28-9)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere

2: trimethylsilylazide / acetonitrile / 17 h / 20 °C / Inert atmosphere

With trimethylsilylazide; triethylamine; In tetrahydrofuran; acetonitrile;

DOI:10.1039/c1dt10898k

upstream raw materials:

C₁₃H₁₉Cl₃N₂Si

C₂₂H₂₅Cl₂N₃OSi