8-methylnonanoic acid 2-(4-hydroxy-3-methoxyphenyl)ethyl ester

Base Information

• Chemical Name: 8-methylnonanoic acid 2-(4-hydroxy-3-methoxyphenyl)ethyl ester
• CAS No.: 951221-74-2
• Molecular Formula: C₁₉H₃₀O₄
• Molecular Weight: 322.445
• Mol file: 951221-74-2.mol

Synonyms:8-methylnonanoic acid 2-(4-hydroxy-3-methoxyphenyl)ethyl ester

Chemical Property of 8-methylnonanoic acid 2-(4-hydroxy-3-methoxyphenyl)ethyl ester

Chemical Property:

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Technology Process of 8-methylnonanoic acid 2-(4-hydroxy-3-methoxyphenyl)ethyl ester

There total 1 articles about 8-methylnonanoic acid 2-(4-hydroxy-3-methoxyphenyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

8-methylnonanoic acid (5963-14-4) + homovanillyl alcohol (2380-78-1) → 8-methylnonanoic acid 2-(4-hydroxy-3-methoxyphenyl)ethyl ester (951221-74-2)

Guidance literature:

novozyme 435; at 50 ℃; for 16h; Enzymatic reaction; Neat (no solvent);

Reference yield:

8-methylnonanoic acid 2-(4-hydroxy-3-methoxyphenyl)ethyl ester (951221-74-2) + 2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-D-glucopyranose (18464-08-9,66073-13-0,71623-44-4,101981-29-7,109922-72-7,109922-73-8,132287-75-3,132287-76-4,132287-78-6,132303-63-0,134311-82-3,134333-39-4) → C45H64O21 + C45H64O21

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20 ℃; for 14h; Overall yield = 46 %; Overall yield = 1.01 g; Inert atmosphere; Cooling with ice;

upstream raw materials:

8-methylnonanoic acid

homovanillyl alcohol

Refernces