methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate

Base Information

Chemical Name:methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate
CAS No.:1295298-30-4
Molecular Formula:C₂₅H₂₂FN₅O₅S
Molecular Weight:523.545
Hs Code.:

Synonyms:methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate

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Chemical Property of methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate

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Technology Process of methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate

There total 1 articles about methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1295298-12-2
1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carboxylic acid [1-(6-bromopyridin-3-yl)cyclopropyl]amide

: 90030-48-1
sodium 3-methoxy-3-oxo-propane-1-sulfinate

: 1295298-30-4
methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate

Guidance literature:: 1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carboxylic acid [1-(6-bromopyridin-3-yl)cyclopropyl]amide; sodium 3-methoxy-3-oxo-propane-1-sulfinate; copper(l) iodide; In dimethyl sulfoxide; at 110 ℃; for 2h; Inert atmosphere; Microwave irradiation;

With ammonium chloride; In water; dimethyl sulfoxide; ethyl acetate;

With sodium hydrogencarbonate; In water; dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 1295298-30-4
methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate

: 1295298-32-6
1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carboxylic acid [1-(6-sulfamoylpyridin-3-yl)cyclopropyl]amide

Guidance literature:: methyl 3-[5-(1-{[1-(4-fluorophenyl)-1H-pyrazolo[3,4-c]pyridine-4-carbonyl]amino}cyclopropyl)pyridine-2-sulfonyl]propionate; With sodium methylate; In methanol; dimethyl sulfoxide; for 0.25h;

With sodium acetate; hydroxylamine-O-sulfonic acid; In methanol; water; dimethyl sulfoxide; at 20 ℃; for 60h; Cooling with water bath;

With sodium hydrogencarbonate; In methanol; water; dimethyl sulfoxide; ethyl acetate; pH=7;