1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Base Information

Chemical Name:1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane
CAS No.:1621595-74-1
Molecular Formula:C₂₃H₂₆B₁₀N₂O₂
Molecular Weight:470.582
Hs Code.:

Synonyms:1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

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Technology Process of 1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

There total 3 articles about 1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1621595-64-9
1-(4-aminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

: 501-53-1,94274-21-2
benzyl chloroformate

: 1621595-74-1
1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.ejmech.2014.07.034

Reference yield:

: 1621595-62-7
1-(4-cyanophenyl)-2-(4-nitrophenyl)-1,2-dicarba-closo-dodecaborane

: 1621595-74-1
1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: Multi-step reaction with 2 steps

1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; tetrahydrofuran / 3 h / 20 °C

2: sodium hydrogencarbonate / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

With 10 wt% Pd(OH)2 on carbon; hydrogen; sodium hydrogencarbonate; In tetrahydrofuran; ethanol;
DOI:10.1016/j.ejmech.2014.07.034

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1621595-74-1
1-(4-benzyloxycarbonylaminophenyl)-2-(4-cyanophenyl)-1,2-dicarba-closo-dodecaborane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol; tetrahydrofuran / 3 h / 20 °C

3.1: sodium hydrogencarbonate / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

With 10 wt% Pd(OH)2 on carbon; hydrogen; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.07.034