3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

Base Information

Chemical Name:3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal
CAS No.:1013941-14-4
Molecular Formula:C₃₂H₃₉N₃O₃
Molecular Weight:513.68
Hs Code.:

3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

Synonyms:3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

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Chemical Property of 3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

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Technology Process of 3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

There total 1 articles about 3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1013941-13-3
3-benzyloxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

: 1013941-14-4
3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

Guidance literature:: With ammonium formate; palladium 10% on activated carbon; In methanol; at 90 ℃; for 0.05h; Microwave irradiation;

Reference yield: 73.0%

: 1013941-14-4
3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal

: 3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one

Guidance literature:: 3-hydroxy-15-[3-(4-p-tolyl-[1,2,3]triazol-1-yl)-propyl]-13-methyl-6,7,8,9,11,12,13,14,15,16-decahydro-cyclopenta[a]phenanthren-17-one ethylene glycol acetal; With o-toluenesulfonic acid; water; In methanol; acetone; at 150 ℃; for 0.0833333h; Microwave irradiation;

With sodium hydrogencarbonate; In water;