N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide

Base Information

Chemical Name:N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide
CAS No.:99632-48-1
Molecular Formula:BrH*C₁₄H₂₂BrNO₂
Molecular Weight:397.15
Hs Code.:

Synonyms:N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide

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Chemical Property of N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide

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Technology Process of N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide

There total 3 articles about N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 99632-43-6
N-n-propyl-1-(2,5-dimethoxyphenyl)-2-aminopropane

: 99632-48-1
N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide

Guidance literature:: With hydrogen bromide; bromine; In acetic acid; for 3h; Ambient temperature;
DOI:10.1021/jm00152a005

Reference yield:

: 2801-68-5
2,5-dimethoxyphenylisopropylamine

: 99632-48-1
N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: 27 percent / sodium bicarbonate / CHCl₃ / 18 h / Ambient temperature

2: 81 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

3: 85 percent / Br₂, 48percent HBr / acetic acid / 3 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen bromide; bromine; sodium hydrogencarbonate; In tetrahydrofuran; chloroform; acetic acid;
DOI:10.1021/jm00152a005

Reference yield:

: 99632-44-7
N-propionyl-1-(2,5-dimethoxyphenyl)-2-aminopropane

: 99632-48-1
N-n-propyl-1-(2,5-dimethoxy-4-bromophenyl)-2-aminopropane hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / LiAlH₄ / tetrahydrofuran / 4 h / Heating

2: 85 percent / Br₂, 48percent HBr / acetic acid / 3 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen bromide; bromine; In tetrahydrofuran; acetic acid;
DOI:10.1021/jm00152a005