N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Base Information

Chemical Name:N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide
CAS No.:1401456-74-3
Molecular Formula:C₂₆H₂₈N₆O₆S₂
Molecular Weight:584.677
Hs Code.:

Synonyms:N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

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Chemical Property of N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

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Technology Process of N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

There total 3 articles about N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 526193-77-1
2,2'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(methan-1-yl-1-ylidene)bis (hydrazinecarbothioamide)

: 108-24-7
acetic anhydride

: 1401456-74-3
N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Guidance literature:: for 10h; Reflux;
DOI:10.1016/j.saa.2012.06.030

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 1401456-74-3
N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 4 h / Reflux

2: hydrogenchloride / ethanol; water / 4 h / Reflux

3: 10 h / Reflux

With hydrogenchloride; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.saa.2012.06.030

Reference yield:

: 83169-98-6
3,3'-[ethane-1,2-diylbis(oxy)]dibenzaldehyde

: 1401456-74-3
N,N'-(5,5'-(3,3'-(ethane-1,2-diylbis(oxy))bis(3,1-phenylene))bis(4-acetyl-4,5-dihydro-1,3,4-thiadiazole-5,2-diyl))diacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol; water / 4 h / Reflux

2: 10 h / Reflux

With hydrogenchloride; In ethanol; water;
DOI:10.1016/j.saa.2012.06.030