Technology Process of (E)-(4-methyldeca-1,5-dien-4-yl)benzene
There total 4 articles about (E)-(4-methyldeca-1,5-dien-4-yl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(allylPdCl)2; o-phenylenebis(diphenylphosphine); water; cesium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/ol500456s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride; sodium methylate / tetrahydrofuran / 1.5 h / 60 °C
2: salicylic acid / water; acetonitrile / 10 h / 80 °C
3: dmap; triethylamine / dichloromethane / 1 h / 20 °C
4: (allylPdCl)2; o-phenylenebis(diphenylphosphine); cesium fluoride; water / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
With
dmap; lithium aluminium tetrahydride; (allylPdCl)2; o-phenylenebis(diphenylphosphine); water; sodium methylate; triethylamine; cesium fluoride; salicylic acid;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1021/ol500456s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: salicylic acid / water; acetonitrile / 10 h / 80 °C
2: dmap; triethylamine / dichloromethane / 1 h / 20 °C
3: (allylPdCl)2; o-phenylenebis(diphenylphosphine); cesium fluoride; water / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere
With
dmap; (allylPdCl)2; o-phenylenebis(diphenylphosphine); water; triethylamine; cesium fluoride; salicylic acid;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1021/ol500456s
