H-Gly-(S)-NHC(CH₃)((E)-CH=CHCH₂NHC(=NH)NH₂)C(O)-Ala-Phe-Val-Thr-Ile-Gly-Lys-OH

Base Information

• Chemical Name: H-Gly-(S)-NHC(CH₃)((E)-CH=CHCH₂NHC(=NH)NH₂)C(O)-Ala-Phe-Val-Thr-Ile-Gly-Lys-OH
• CAS No.: 916161-83-6
• Molecular Formula: C₄₄H₇₃N₁₃O₁₁
• Molecular Weight: 960.144
• Mol file: 916161-83-6.mol

Synonyms:H-Gly-(S)-NHC(CH₃)((E)-CH=CHCH₂NHC(=NH)NH₂)C(O)-Ala-Phe-Val-Thr-Ile-Gly-Lys-OH

Chemical Property of H-Gly-(S)-NHC(CH₃)((E)-CH=CHCH₂NHC(=NH)NH₂)C(O)-Ala-Phe-Val-Thr-Ile-Gly-Lys-OH

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of H-Gly-(S)-NHC(CH₃)((E)-CH=CHCH₂NHC(=NH)NH₂)C(O)-Ala-Phe-Val-Thr-Ile-Gly-Lys-OH

There total 1 articles about H-Gly-(S)-NHC(CH₃)((E)-CH=CHCH₂NHC(=NH)NH₂)C(O)-Ala-Phe-Val-Thr-Ile-Gly-Lys-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

(E,2S)-2-{[(N-tert-butoxycarbonyl)glycyl]amino}-5-{[(tert-butoxycarbonyl)amino-(tert-butoxycarbonylimino)methyl]amino}-2-methylpent-3-enoic acid (916161-80-3) → H-Gly-(S)-NHC(CH3)((E)-CH=CHCH2NHC(=NH)NH2)C(O)-Ala-Phe-Val-Thr-Ile-Gly-Lys-OH (916161-83-6)

Guidance literature:

(E,2S)-2-{[(N-tert-butoxycarbonyl)glycyl]amino}-5-{[(tert-butoxycarbonyl)amino-(tert-butoxycarbonylimino)methyl]amino}-2-methylpent-3-enoic acid; H₂N-AFVTIGK-resin-bound; With dmap; dicyclohexyl-carbodiimide; In dimethyl sulfoxide; at 60 ℃; for 48h;

With chlorotriisopropylsilane; trifluoroacetic acid; In water; phenol; at 20 ℃; for 2h; Further stages.;

DOI:10.1039/b611170j

upstream raw materials:

(E,2S)-2-{[(N-tert-butoxycarbonyl)glycyl]amino}-5-{[(tert-butoxycarbonyl)amino-(tert-butoxycarbonylimino)methyl]amino}-2-methylpent-3-enoic acid