1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Base Information

Chemical Name:1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene
CAS No.:93622-56-1
Molecular Formula:C₃₄H₃₉NO₆
Molecular Weight:557.687
Hs Code.:

Synonyms:1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Suppliers and Price of 1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Chemical Property:

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Technology Process of 1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

There total 8 articles about 1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 148-24-3,24804-14-6
8-quinolinol

: 93622-55-0
1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-(3-chloropropoxy)-4-t-butylbenzene

: 93622-56-1
1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 70 ℃; for 48h;
DOI:10.1246/bcsj.57.1976

Reference yield:

: 148-24-3,24804-14-6
8-quinolinol

: 93622-56-1
1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) t-BuOK / 1.) DMSO; 2.) 70 deg C, 38 h

2: 68 percent / thionyl chloride / benzene / 5 h / Heating

3: 1.) t-BuOK; 2.) KI / 1.) DMSO; 2.) 70 deg C, 4 d

With thionyl chloride; potassium tert-butylate; potassium iodide; In benzene;
DOI:10.1246/bcsj.57.1976

Reference yield:

: 5263-93-4
3-(8-quinolyloxy)-1-propanol

: 93622-56-1
1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / thionyl chloride / benzene / 5 h / Heating

2: 1.) t-BuOK; 2.) KI / 1.) DMSO; 2.) 70 deg C, 4 d

With thionyl chloride; potassium tert-butylate; potassium iodide; In benzene;
DOI:10.1246/bcsj.57.1976