p-tolyl 1-azidoethyl sulfide

Base Information

Chemical Name:p-tolyl 1-azidoethyl sulfide
CAS No.:108795-78-4
Molecular Formula:C₉H₁₁N₃S
Molecular Weight:193.272
Hs Code.:

Synonyms:p-tolyl 1-azidoethyl sulfide

Suppliers and Price of p-tolyl 1-azidoethyl sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 1-azidoethyl sulfide

Chemical Property:

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Technology Process of p-tolyl 1-azidoethyl sulfide

There total 2 articles about p-tolyl 1-azidoethyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59480-99-8
1-(1-Chloro-ethylsulfanyl)-4-methyl-benzene

: 108795-78-4
p-tolyl 1-azidoethyl sulfide

Guidance literature:: With sodium azide; In ethanol; water; at 25 ℃; for 1.5h; Yield given;
DOI:10.1021/jo00391a062

Reference yield:

: 622-63-9
ethyl p-tolyl sulfide

: 108795-78-4
p-tolyl 1-azidoethyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: N-chlorosuccinimide / CCl₄ / 5 h / 25 °C

2: NaN₃ / ethanol; H₂O / 1.5 h / 25 °C

With N-chloro-succinimide; sodium azide; In tetrachloromethane; ethanol; water;
DOI:10.1021/jo00391a062