N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide
CAS No.:1245035-60-2
Molecular Formula:C₂₈H₃₂ClN₃O₃S
Molecular Weight:526.099
Hs Code.:

Synonyms:N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

There total 5 articles about N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-13-2
4-Butylaniline

: C₁₈H₁₈Cl₂N₂O₃S

: 1245035-60-2
N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2013.01.028

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 1245035-60-2
N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: chlorosulfonic acid / 2 h / 50 °C

2: thionyl chloride / 16 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With chlorosulfonic acid; thionyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.tet.2013.01.028

Reference yield:

: 89001-57-0
5-(chlorosulfonyl)-2-methylbenzenecarboxylic acid

: 1245035-60-2
N-(4-butylphenyl)-3-(4-(2-chlorophenyl)piperazine-1-carbonyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 16 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.tet.2013.01.028